Experimental analysis of carbon content in carbon steel by laser induced plasma spectroscopy method

Abstract

Abstract:

Laser induced plasmas spectroscopy (LIPS) has acquired great interest in recent years as a new method of elemental analysis, qualitative information about the elemental composition of an object can be rapidly obtained using LIPS. In the experiment, laser induced plasma spectroscopy (LIPS) was used to determine the carbon content in carbon steel. The plasma was formed by focusing a Nd: YAG laser on the sample surface. By the optical emission spectroscopy of the plasma, the 193.09nm C line was selected to be determined. The calibration curve was obtained, and the detection limit was within 460ppm. The results show that this technique can be applied for direct composition determination in steel analysis.

Key words: spectroscopy, laser induced plasma spectroscopy, quantitative analysis, calibration curve, carbon steel

CLC Number:

O433.59

FEI Teng, WANG Qiu-ping, LU Xian-yang, WANG Sheng-bo, PAN Cong-yuan. Experimental analysis of carbon content in carbon steel by laser induced plasma spectroscopy method[J]. J4, 2012, 29(2): 209-214.

References

[1]Aragón C, Aguilera J A. Characterization of laser induced plasmas by optical emission spectroscopy: A review of experiments and methods [J]. Spectrochimica Acta Part B, 2008, 63(9):893-916
[2] Song Dongting，Qi Hongxing，Shu Rong. Quantitative analysis of heavy metal in soil by laser-induced breakdown spectroscopy [J].Science Technology and Engineering, 2008, 8(15): 4070-4077(in Chinese).
[3] Laszlo Peter, Volker Sturm, and Reinhard Noll, Liquid steel analysis with laser-induced breakdown spectrometry in the vacuum ultraviolet, 2003, Vol. 42, No. 30:6199-6204 , APPLIED OPTICS
[4] LI Jing ，ZHAI Chao，ZHANG Shi-ding，ZHANG Jian-qiu ，MENG Xiang-ru. Determination of Minor Elements in Stainless Steel by Laser-Induced Plasma Spectroscopy (LIPS). Spectroscopy and Spectral Analysis, 2008, Vol.28，No.4:930-933(in Chinese)
[5] Awadhesh K. Rai, Fang Y. Yueh, and Jagdish P. Singh. High temperature fiber optic laser-induced breakdown spectroscopy sensor for analysis of molten alloy constituents, REVIEW OF SCIENTIFIC INSTRUMENTS, 2002, Vol.73, No.10:3589-3599
[6] Palanco S, Conesa S, and Laserna J. J. Analytical control of liquid steel in an induction melting furnace using a remote laser induced plasma spectrometer, J. Anal. At. Spectrom, 2004, 19,462–467
[7] Pasquini C , Cortez J, Silva L.M.C, Gonzaga F.B, Laser induced breakdown spectroscopy, J. Braz. Chem. Soc. 18 (2007) 463–512.
[8] CIUCCI A , CORSI M , PALLESCHI V, RASTELLI S, SALVETTI A, and TOGNONI E, New Procedure for Quantitative Elemental Analysis by Laser-Induced Plasma Spectroscopy, Applied spectroscopy, Volume 53, Number 8:960-964, 1999
[9] Walid Tawfik Y. Mohamed, Improved LIBS limit of detection of Be, Mg, Si, Mn, Fe and Cu in aluminum alloy samples using a portable Echelle spectrometer with ICCD camera, Optics & Laser Technology 40 (2008) :30–38
[10]NIST Atomic Spectra Database, http://www.nist.gov/pml/data/asd.cfm

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